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• {SNA} Analytical Standards, E-G, 农残和代谢标准品, 分析/色谱, 按照字母排序
• {SNA} All alphabetically sorted, Alphabetic, Analytical Standards, Analytical/Chromatography, Chromatography, E-G, Environmental Standards, F, FA - FL, Pesticides & Metabolites
• {SNA} Analytical Standards,
• {SNA} All alphabetically sorted, Al
• {SNA} Alphabetical Index of Analytical Standards, Analytical Standards, Analytical/Chromatography, Chromatography, E-G, Environmental Standards, F, FA - FL, 农残和代谢标准品, 按照字母排序
• {uni_hamburg} no charge; carbocycle; aromatic; 6RingOnly; 6ring; 1fragment

相关文献及参考

• Short: III/20a Title: Nuclear Quadrupole Resonance Spectroscopy Data: Nuclei D ... Cl Author: Chihara, H.; Nakamura, N. Editor: Hellwege, K.-H.; Hellwege, A.M. Source: Landolt-Börnstein, New Series Volume: III/20a Year: 1988 Keyword: NQR ISBN: 3-540-18161-X ISBN: 978-3-540-18161-3 Internet Resource: DOI:10.1007/b31153 RefComment: IX,677 pages. Hardcover Abstract: Nuclear Quadrupole Resonance Spectroscopy has become a standard method for structural research in molecular and solid state physics as well as for different branches of chemistry. The volumes cover data for more than 8,000 substances in the solid state. Data for free molecules have been published in volumes II/14 and II/15 of the New Series. The tables are arranged according to the atomic number of the elements.
• Short: III/35E Title: Nuclear Magnetic Resonance (NMR) Data: Chemical Shifts for Oxygen-17 Author: Duddeck, H.; Toth, G.; Simon, A. Editor: Gupta, R.R.; Lechner, M.D. Source: Landolt-Börnstein, New Series Volume: III/35E Year: 2002 Keyword: Alipathic and Aromatic hydrocarbons; Coupling constant j; Nuclear Magnetic Resonance; chemical shifts δ ISBN: 3-540-42501-2 ISBN: 978-3-540-42501-4 Internet Resource: DOI:10.1007/b92953 RefComment: VII, 230 pages. With CD-ROM., Hardcover Abstract: This volume provides a comprehensive and evaluated compilation of nuclear magnetic resonance data. Chemical shifts and coupling constants of boron-11 and phosphorus-31 (subvol. A), fluorine-19 and nitrogen-15 (subvol. B), hydrogen-1 (subvol. C), carbon-13 (subvol. D), and oxygen-17 (subvol. E) compounds are tabulated together with the gross- and structure formulas and the most readily available solvents. Due to the large amount of the data merely chemical shifts are presented in the printed versions, and all the data, chemical shifts and coupling constants are provided on CD-ROM's.
• Short: III/5a Title: Structure Data of Organic Crystals: C ... C 13 Author: Schudt, E.; We

安全信息

GHS Symbol

TYPE OF TEST            : LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE       : Administration onto the skin
SPECIES OBSERVED        : Rodent - rabbit
DOSE/DURATION           : 1350 mg/kg
TOXIC EFFECTS :
   Details of toxic effects not reported other than lethal dose value
REFERENCE :
   85JFAN "Agrochemicals Handbook," with updates, Hartley, D., and H. Kidd,
   eds., Nottingham, Royal Soc. of Chemistry, 1983-86 Volume(issue)/page/year:
   A195,1983

TYPE OF TEST            : LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE       : Intraperitoneal
SPECIES OBSERVED        : Rodent - rat
DOSE/DURATION           : 940 mg/kg
TOXIC EFFECTS :
   Details of toxic effects not reported other than lethal dose value
REFERENCE :
   85JFAN "Agrochemicals Handbook," with updates, Hartley, D., and H. Kidd,
   eds., Nottingham, Royal Soc. of Chemistry, 1983-86 Volume(issue)/page/year:
   A195,1983

TYPE OF TEST            : LDLo - Lowest published lethal dose
ROUTE OF EXPOSURE       : Subcutaneous
SPECIES OBSERVED        : Rodent - rabbit
DOSE/DURATION           : 275 mg/kg
TOXIC EFFECTS :
   Gastrointestinal - other changes
   Kidney, Ureter, Bladder - other changes
REFERENCE :
   AEXPBL Archiv fuer Experimentelle Pathologie und Pharmakologie.  (Leipzig,
   Ger. Dem. Rep.)  V.1-109, 1873-1925.  For publisher information, see NSAPCC.
    Volume(issue)/page/year: 35,401,1895

TYPE OF TEST            : LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE       : Oral
SPECIES OBSERVED        : Rodent - mouse
DOSE/DURATION           : 515 mg/kg
TOXIC EFFECTS :
   Gastrointestinal - other changes
   Liver - other changes
REFERENCE :
   KYDKAJ Kyoritsu Yakka Daigaku Kenkyu Nenpo.  Annual Report of the Kyoritsu
   College of Pharmacy. (Kyoritsu Yakka Daigaku, 1-5-30 Shibakoen Minato-ku,
   Tokyo, Japan)  V.1-    1955-

TYPE OF TEST            : LDLo - Lowest published let

TYPE OF TEST            : Morphological transformation
TEST SYSTEM             : Rodent - hamster Kidney
DOSE/DURATION           : 33400 ug/L
REFERENCE :
   PMRSDJ Progress in Mutation Research.  (Elsevier Science Pub. Co., Inc., 52
   Vanderbilt Ave., New York, NY 10017)  V.1-    1981- Volume(issue)/page/year:
   1,626,1981

TYPE OF TEST            : Micronucleus test
ROUTE OF EXPOSURE       : Intraperitoneal
TEST SYSTEM             : Rodent - mouse
DOSE/DURATION           : 6400 ug/kg
REFERENCE :
   PMRSDJ Progress in Mutation Research.  (Elsevier Science Pub. Co., Inc., 52
   Vanderbilt Ave., New York, NY 10017)  V.1-    1981- Volume(issue)/page/year:
   1,686,1981

TYPE OF TEST            : Mutation in microorganisms
TEST SYSTEM             : Yeast - Saccharomyces cerevisiae
DOSE/DURATION           : 250 mg/L
REFERENCE :
   PMRSDJ Progress in Mutation Research.  (Elsevier Science Pub. Co., Inc., 52
   Vanderbilt Ave., New York, NY 10017)  V.1-    1981-

TYPE OF TEST            : Mutation in microorganisms
TEST SYSTEM             : Bacteria - Salmonella typhimurium
DOSE/DURATION           : 10 ug/plate
REFERENCE :
   PMRSDJ Progress in Mutation Research.  (Elsevier Science Pub. Co., In

TYPE OF TEST            : Mutation in microorganisms
TEST SYSTEM             : Bacteria - Escherichia coli
DOSE/DURATION           : 50 ug/plate
REFERENCE :
   PMRSDJ Progress in Mutation Research.  (Elsevier Science Pub. Co., Inc., 52
   Vanderbilt Ave., New York, NY 10017)  V.1-    1981- Volume(issue)/page/year:
   1,351,1981

TYPE OF TEST            : Gene conversion and mitotic recombination
TEST SYSTEM             : Yeast - Saccharomyces cerevisiae
DOSE/DURATION           : 196 ppm
REFERENCE :
   PMRSDJ Progress in Mutation Research.  (Elsevier Science Pub. Co., Inc., 52
   Vanderbilt Ave., New York, NY 10017)  V.1-    1981- Volume(issue)/page/year:
   1,481,1981

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其他信息

• TCI Shanghai:1-氧化二苯基二氮烯 Azoxybenzene,>;98.0%(T)(495-48-7)
• 急性毒性:口服-大鼠 LD50: 620 毫克/公斤; 口服-小鼠 LD50; 515 毫克/公斤
• Sigma Aldrich:495-48-7(sigmaaldrich)
• Acros Organics:Azoxybenzene, 97%(495-48-7)
• 毒性分级:中毒
• 上游原料:D-无水葡萄糖 --> 滤纸
• 用途一:有机合成中间体。
• 类别:易燃液体
• 储运特性:通风低温干燥
• 可燃性危险特性:较易燃; 燃烧产生有毒氮氧化物烟雾
• 图谱信息:1-氧化二苯基二氮烯 (495-48-7)质谱(MS) 1-氧化二苯基二氮烯 (495-48-7)红外图谱(IR2) 1-氧化二苯基二氮烯 (495-48-7)核磁图( 1 HNMR) 1-氧化二苯基二氮烯 (495-48-7)核磁图( 13 CNMR) 1-氧化二苯基二氮烯 (495-48-7)红外图谱(IR1)
• 方法一:硝基苯经还原而得。在反应锅内投入硝基苯、氢氧化钠溶液，升温至60℃，慢慢加入葡萄糖液，在65-75℃下保温1h，即反应生成氧化偶氮苯。实验室制备实例：在带回流装置的500ml烧瓶中，加入30g氢氧化钠和100ml水配成的溶液，再加入20.5g纯的硝基苯，在水浴中加热，温度保持在55-60℃。在搅拌下分多次加入总量为21g的无水葡萄糖，约1h加完。在沸水浴中加热2h。然后将热的反应物进行水蒸气蒸馏，除去未反应的硝基苯和反应副产物苯胺。当馏出液呈澄清时（约蒸出1L），将剩余物倒入烧杯中，冰浴冷却。反应物很快凝固，将其研碎、水洗，在滤纸上晾干，得13g纯品，熔点35-35.5℃，产率79%，有乙醇重结晶，熔点为36℃。
• Alfa Aesar:氧化偶氮苯,98+% Azoxybenzene, 98+%(495-48-7)
• MOL 文件:495-48-7.mol
• 刺激数据:皮肤-兔子 10 毫克/24小时 轻度; 眼睛-兔子