2-Hydroxy-4-methylquinoline 2-羟基-4-甲基喹啉

CAS 607-66-9 MFCD00006745

化学结构图

607-66-9
SMILES: CC1C=C(O)N=C2C=CC=CC2=1

化学属性

Mol. FormulaC10H9NO
Mol. Weight159.18
Melting Point221-223 °C
TSCANo
Appearance 针状体结晶。熔点245℃，沸点>;360，270℃（2.27kPa）。溶于乙醇和热水，微溶于冷水、乙醚、氯仿和苯。
Boiling Point284.68 °C at 760 mmHg

别名和识别编码

Chemical Name2-Hydroxy-4-methylquinoline
CAS Number607-66-9
Alfabeta NameMETHYLQUINOLINOL 42---
MDL NumberMFCD00790771
Synonym 4-Methylquinolin-2(1H)-one {LY} 4-Methylquinolin-2(1H)-one {} {LY} 4-Methylquinolin-2(1H)-one {} {} {LY} 4-Methylquinolin-2(1H)-one {} {} {} {LY} 4-Methylquinolin-2(1H)-one {} {} {} {} {LY} 4-Methylquinolin-2(1H)-one {} {} {} {} {} {LY} 4-Methylquinolin-2(1H)-one {} {} {} {} {} {} {} {} {} {} {} {} {LY} 4-Methylquinolin-2(1H)-one {} {} {} {} {} {} {} {LY} 4-Methylquinolin-2(1H)-one {} {} {} {} {} {} {} {} {LY} 4-Methylquinolin-2(1H)-one {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {LY} 4-Methylquinolin-2(1H)-one {} {} {} {} {} {} {} {} {} {} {LY} 4-Methylquinolin-2(1H)-one {} {} {} {} {} {} {} {} {} {} {} { {} {} {} {} {} {} {} {} {} {} {} {LY} 4-Methylquinolin-2(1H)-one {} {} {} {} {} {} {} {} {} {} {} {} {LY} 4-Methylquinolin-2(1H)-one {} {} {} {} {} {} {} {} {} {} {} {} {} {LY} 4-Methylquinolin-2(1H)-one {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {LY} 4-Methylquinolin-2(1H)-one {} {} {} {} {} {} {} {} {} {}
PubChem Substance ID87570686
EC Number210-139-0
Beilstein Registry Number21,107
Chemical Name Translation2-羟基-4-甲基喹啉
Reaxys-RN1525906
InChIKeyAPLVPBUBDFWWAD-UHFFFAOYSA-N
Canonical SMILESO=C1NC2=C(C=CC=C2)C(C)=C1.[607-66-9]
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分类

  • {SNA} Building Blocks, C8 to C10, Chemical Synthesis, Heterocyclic Building Blocks, Quinolines

安全信息

Warnings IRRITANT
WGK Germany3
GHS Symbol
Precautionary statements
  • P261 Avoid breathing dust/fume/gas/mist/vapours/spray. 避免吸入粉尘/烟/气体/烟雾/蒸汽/喷雾。
  • P264 Wash hands thoroughly after handling. 处理后要彻底洗净双手。
  • P280 Wear protective gloves/protective clothing/eye protection/face protection. 戴防护手套/防护服/眼睛的保护物/面部保护物。
  • P302+P350
  • P302+P352+P332+P313+P362+P364
  • P305+P351+P338
  • P305+P351+P338+P337+P313
  • P332+P313
  • P337+P313
  • P362 Take off contaminated clothing and wash before reuse. 脱掉污染的衣服，清洗后方可重新使用
Hazard statements
  • H315 Causes skin irritation 会刺激皮肤
  • H319 Causes serious eye irritation 严重刺激眼睛
  • H335 May cause respiratory irritation 可能导致呼吸道刺激
Signal word Warning
Personal Protective Equipment dust mask type N95 (US), Eyeshields, Gloves
Safety Statements
  • S37/39 Wear suitable gloves and eye/face protection 穿戴适当的手套和眼睛/面保护；
  • S26 In case of contact with eyes, rinse immediately with plenty of water and seek medical advice 眼睛接触后，立即用大量水冲洗并征求医生意见；
  • S37 Wear suitable gloves 戴适当手套；
  • S22 Do not breathe dust 不要吸入粉尘；
  • S36/37/39 Wear suitable protective clothing, gloves and eye/face protection 穿戴适当的防护服、手套和眼睛/面保护；
Risk Statements
  • R36/37/38 Irritating to eyes, respiratory system and skin 对眼睛、呼吸系统和皮肤有刺激性
  • R20/21/22 Harmful by inhalation, in contact with skin and if swallowed 吸入、皮肤接触和不慎吞咽有害
Hazard Codes Xi Xi,Xn
Storage condition 2-8°C {LY} 2-8°C {} {LY} 2-8°C {} {} {LY} 2-8°C {} {} {} {LY} 2-8°C {} {} {} {} {LY} 2-8°C {} {} {} {} {} {LY} 2-8°C {} {} {} {} {} {} {LY} 2-8°C {} {} {} {} {} {} {} {LY} 2-8°C {} {} {} {} {} {} {} {} {LY} 2-8°C {} {} {} {} {} {} {} {} {} {LY} 2-8°C {} {} {} {} {} {} {} {} {} {} {LY} 2-8°C {} {} {} {} {} {} {} {} {} {} {} {LY} 2-8°C {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {LY} 2-8°C {} {} {} {} {} {} {} {} {} {} {} {} {} { {} {} {} {} {} {} {} {} {} {} {} {} {} {LY} 2-8°C {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {LY} 2-8°C {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {LY} 2-8°C {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} { {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {LY} 2-8°C {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} { {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {LY} 2-8°C {} {} {} {} {} {} {} {} {} {} {}

其他信息

  • 图谱信息:2-羟基-4-甲基喹啉(607-66-9)红外图谱(IR2) 2-羟基-4-甲基喹啉(607-66-9)红外图谱(IR1) 2-羟基-4-甲基喹啉(607-66-9)核磁图( 1 HNMR) 2-羟基-4-甲基喹啉(607-66-9)质谱(MS)
  • Acros Organics:2-羟基-4-甲基喹啉 2-Hydroxy-4-methylquinoline, 97%(607-66-9)
  • TCI Shanghai:4-甲基喹诺酮 4-Methylcarbostyril,>;98.0%(T)(607-66-9)
  • Alfa Aesar:2-羟基-4-甲基喹啉,98% 2-Hydroxy-4-methylquinoline, 98%(607-66-9)
  • 用途一:用作有机合成中间体。
  • 下游产品:4-甲基-2-氯-喹啉
  • 上游原料:乙醇 --> N-乙酰乙酰苯胺
  • 方法一:由乙酰乙酰苯胺在硫酸存在下环合而得。将浓硫酸预热至75℃，分批加入乙酰乙酰苯胺，控制温度为70-75℃。加料结束后将温度升至95℃，反应15min后冷却至65℃，将混合物倒入水中。冷却后过滤，用水和甲醇洗涤产物，干燥后用95%乙醇重结晶即得成品。
  • Sigma Aldrich:607-66-9(sigmaaldrich)
  • 2-羟基-4-甲基喹啉价格(试剂级):更新日期 产品编号 产品名称 包装 价格 2014/06/02 H0259 4-甲基喹诺酮 4-Methylcarbostyril 25G 662元 2010/06/21 AC12157EA 2-羟基-4-甲基喹啉 4-methyl-2-quinolinol 10 GR 480元 2010/06/21 AC12157EE 2-羟基-4-甲基喹啉 4-methyl-2-quinolinol 50 GR 2070元
  • MOL 文件:607-66-9.mol

系列性分类

  1. Chemical Synthesis 化学合成
  2. Building Blocks 合成砌块
  3. Heterocyclic Building Blocks 杂环合成砌块
  4. Isoquinolines 异喹啉
  1. Chemical Synthesis 化学合成
  2. Building Blocks 合成砌块
  3. Heterocyclic Building Blocks 杂环合成砌块
  4. Quinaldines 奎纳丁
  1. Chemical Synthesis 化学合成
  2. Building Blocks 合成砌块
  3. Heterocyclic Building Blocks 杂环合成砌块
  4. Quinolines 喹啉
  1. Chemical Synthesis 化学合成
  2. Building Blocks 合成砌块
  3. Heterocyclic Building Blocks 杂环合成砌块
  4. Quinolines 喹啉
  5. C8 to C10 - Quinolines

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