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分类

• {SNA} Building Blocks, Chemical Synthesis, Nitrogen Compounds, Organic Building Blocks, Protected Amines
• {uni_hamburg} no charge; carbocycle; aromatic; 6RingOnly; 6ring; amide; ether; 1fragment

相关文献及参考

• Short: III/35D2 Title: Nuclear Magnetic Resonance (NMR) Data: Chemical Shifts for Carbon-13, Part 2: Aromatic Compounds Author: Mikhova, B. Editor: Gupta, R.R.; Lechner, M.D. Source: Landolt-Börnstein, New Series Volume: III/35D2 Year: 2005 Keyword: aromatic compounds; carbon-13; chemical shift; coupling constant; molecular structure ISBN: 978-3-540-20189-2 ISBN: 3-540-20189-0 Internet Resource: DOI:10.1007/b83345 RefComment: VIII, 291 p., Hardcover RefComment: Written for Science and engineers in the fields of physics, chemistry and physical chemistry who inted to use NMR to study the structure and the binding of molecules Abstract: Nuclear Magnetic Resonance (NMR) is based on the fact that certain nuclei exhibit a magnetic moment, orient by a magnetic field, and absorb characteristic frequencies in the radiofrequency part of the spectrum. The spectral lines of the nuclei are highly influenced by the chemical environment i.e. the structure and interaction of the molecules. NMR is now the leading technique and a powerful tool for the investigation of the structure and interaction of molecules. The present Landolt-Börnstein volume III/35 Nuclear Magnetic Resonance (NMR) Data is therefore of major interest to all scientists and engineers who intend to use NMR to study the structure and the binding of molecules. Volume III/35 "NMR-Data" is divided into several subvolumes and parts. Subvolume III/35A contains the nuclei 11B and 31P, subvolume III/35B contains the nuclei 19F and 15N, subvolume III/35C contains the nucleus 1H, subvolume III/35D contains the nucleus 13C, subvolume III/35E contains the nucleus 17O, and subvolume III/35G contains the nucleus 77Se. More nuclei will be presented later.
• Short: III/35E Title: Nuclear Magnetic Resonance (NMR) Data: Chemical Shifts for Oxygen-17 Author: Duddeck, H.; Toth, G.; Simon, A. Editor: Gupta, R.R.; Lechner, M.D. Source: Landolt-Börnstein, New Series Volume: III/35E Year: 2002 Keywor

安全信息

GHS Symbol

TYPE OF TEST            : LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE       : Oral
SPECIES OBSERVED        : Rodent - mouse
DOSE/DURATION           : 940 mg/kg
TOXIC EFFECTS :
   Details of toxic effects not reported other than lethal dose value
REFERENCE :
   TXAPA9 Toxicology and Applied Pharmacology.  (Academic Press, Inc., 1 E.
   First St., Duluth, MN 55802) V.1-    1959-  Volume(issue)/page/year:
   19,20,1971

其他信息

• 可燃性危险特性:可燃;加热分解释放有毒氮氧化物烟雾
• 2-乙酰氨基苯甲醚价格(试剂级):更新日期 产品编号 产品名称 包装 价格 2014/06/02 A0018 邻乙酰氨基苯甲醚 o-Acetanisidide 500G 2610元 2014/06/02 A0018 邻乙酰氨基苯甲醚 o-Acetanisidide 25G 260元
• 用途一:用于生产红色基B
• 储运特性:库房通风低温干燥
• 图谱信息:2-乙酰氨基苯甲醚(93-26-5)红外图谱(IR2) 2-乙酰氨基苯甲醚(93-26-5)核磁图( 1 HNMR) 2-乙酰氨基苯甲醚(93-26-5)红外图谱(IR1) 2-乙酰氨基苯甲醚(93-26-5)核磁图( 13 CNMR) 2-乙酰氨基苯甲醚(93-26-5)质谱(MS)
• MSDS 信息:o-Acetanisidide(93-26-5).msds
• 毒性分级:中毒
• Sigma Aldrich:93-26-5(sigmaaldrich)
• 用途三:作有机合成原料，用于制造农药，医药等。
• 用途二:作有机合成原料，用于制造农药、医药等。
• 灭火剂:干粉、泡沫、砂土和水
• 急性毒性:口服-小鼠LD50:940毫克/公斤
• 下游产品:N-(4-氨基-2-甲氧基苯基)乙酰胺 --> 菲二啶酮 --> 红色基 ITR --> 耐晒红B盐 --> 2-甲氧基-4-硝基乙酰苯胺 --> 红色基 SW
• 方法一:由邻氨基苯甲醚与乙酐反应得到。将计量的邻氨基苯甲醚投入反应釜，搅拌下加入冰醋酸。在10～12℃滴加乙酐，2h左右加完，静置2h，即得供工业上使用的中间体邻乙酰氨基苯甲醚。配料比为邻氨基苯甲醚：冰醋酸：乙酐＝1：0.9：1（重量比）。也可以将邻氨基苯甲醚与乙酐混合，于沙浴回流2h，放冷，得针状结晶，过滤，用水洗去酸性，再用水重结晶而得成品。
• TCI Shanghai:2-乙酰氨基苯甲醚 o-Acetanisidide,>;98.0%(LC)(T)(93-26-5)
• 类别:有毒物品
• MOL 文件:93-26-5.mol
• 上游原料:邻甲氧基苯胺