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分类

• {uni_hamburg} no charge; alcohol; 1fragment
• {SNA} Alcohols, Building Blocks, C2 to C6, Chemical Synthesis, Organic Building Blocks, Oxygen Compounds

相关文献及参考

• Short: II/25C Title: Structure Data Of Free Polyatomic Molecules: Molecules containing Three or Four Carbon Atoms Author: Graner, G.; Hirota, E.; Iijima, T.; Kuchitsu, K.; Ramsay, D.A.; Vogt, J.; Vogt, N. Editor: Kuchitsu, K. Source: Landolt-Börnstein, New Series Volume: II/25C Year: 2001 Keyword: Free Polyatomic Molecules; Carbon Atoms; Molecules ISBN: 3-540-66774-1 ISBN: 978-3-540-66774-2 Internet Resource: DOI:10.1007/b71431 RefComment: VIII, 481 pages. Hardcover Abstract: This volume contains data on the geometric parameters (internuclear distances, bond angles, dihedral angles of internal rotation etc.) of free polyatomic molecules including free radicals and molecular ions. This survey on structure data is made of four subvolume, each containing the geometric parameters determined in the gas phase either by an analysis of the rotational constants (and sometimes the vibrational constants) obtained from microwave, infrared, Raman, electronic and photoelectron spectroscopy or by an analysis of electron diffraction intensities. Most of the structures listed in the tables are for molecules in the electronic ground state, but structures for electronically excited states have also been included as far as they are available. In this third subvolume, the structure of molecules containing three for four carbon atoms are listed.
• Short: III/38B Title: Refractive Indices of Organic Liquids Author: Wohlfarth, Ch.; Wohlfarth, B. Editor: Lechner, M.D. Source: Landolt-Börnstein, New Series Volume: III/38B Year: 1996 Keyword: organic compounds; refractive index; liquids ISBN: 3-540-60596-7 ISBN: 978-3-540-60596-6 Internet Resource: DOI:10.1007/b85533 RefComment: VII, 4210 pages, Hardcover Abstract: Volume III/38 Optical Constants provides critically evaluated data on refractive indices of inorganic and organic liquids and their wavelength dependence (dispension). Part A contains the inorganic, organometallic, and organononmetallic liquids, and the

安全信息

GHS Symbol

TYPE OF TEST            : TDLo - Lowest published toxic dose
ROUTE OF EXPOSURE       : Intraperitoneal
SPECIES OBSERVED        : Rodent - mouse
DOSE/DURATION           : 3650 mg/kg/8W-I
TOXIC EFFECTS :
   Tumorigenic - neoplastic by RTECS criteria
   Lungs, Thorax, or Respiration - tumors
REFERENCE :
   CNREA8 Cancer Research. (Public Ledger Building, Suit 816, 6th & Chestnut
   Sts., Philadelphia, PA 19106)  V.1-    1941-  Volume(issue)/page/year:
   39,391,1979

TYPE OF TEST            : LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE       : Intraperitoneal
SPECIES OBSERVED        : Rodent - mouse
DOSE/DURATION           : >100 mg/kg
TOXIC EFFECTS :
   Details of toxic effects not reported other than lethal dose value
REFERENCE :
   JOCEAH Journal of Organic Chemistry.  (American Chemical Soc., Distribution
   Office Dept. 223, POB 57136, West End Stn., Washington, DC 20037)  V.1-
   1936-  Volume(issue)/page/year: 21,739,1956

TYPE OF TEST            : LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE       : Oral
SPECIES OBSERVED        : Rodent - mouse
DOSE/DURATION           : 990 mg/kg
TOXIC EFFECTS :
   Behavioral - muscle contraction or spasticity
   Gastrointestinal - ulceration or bleeding from stomach
   Liver - other changes
REFERENCE :
   ZHYGAM Zeitschrift fuer die Gesamte Hygiene und Ihre Grenzgebiete.  (VEB
   Verlag Volk und Gesundheit, Neue Gruenstr. 18, Berlin DDR-1020, Ger. Dem.
   Rep.)  V.1-    1955-  Volume(issue)/page/year: 26,17,1980

其他信息

• 方法一:由四氢呋喃与氯化氢反应而得：在四氢呋喃沸腾的情况下，慢慢通入氯化氢气体。随着反应的进行，反应液温度逐渐升高，直至100℃以上。当温度停留在103.5-105.5℃稳定时，即反应结束。减压分馏，收集80-90℃（1.87kPa）馏分得粗品；再进行减压分馏，收集81-82℃（1.87kPa）馏分得成品，产率为54%-57%。
• Sigma Aldrich:928-51-8(sigmaaldrich)
• 急性毒性:口服-小鼠 LD50: 990 毫克/公斤; 腹腔-小鼠 LD50: >; 100 毫克/公斤
• Alfa Aesar:4-氯-1-丁醇,tech.85% 4-Chloro-1-butanol, tech. 85%(928-51-8)
• 4-氯-1-丁醇价格(试剂级):更新日期 产品编号 产品名称 包装 价格 2014/06/02 C0144 4-氯-1-丁醇(含有数量不等的四氢呋喃) 4-Chloro-1-butanol (contains varying amounts of Tetrahydrofuran) 25G 476元 2014/06/02 C0144 4-氯-1-丁醇(含有数量不等的四氢呋喃) 4-Chloro-1-butanol (contains varying amounts of Tetrahydrofuran) 500G 3310元 2010/06/21 356315000 4-氯-1-丁醇 4-Chloro-1-butanol 85%, balance THF and HCl 500 GR 7467元
• 图谱信息:4-氯-1-丁醇(928-51-8)Raman光谱 4-氯-1-丁醇(928-51-8)质谱(MS) 4-氯-1-丁醇(928-51-8)红外图谱(IR1) 4-氯-1-丁醇(928-51-8)核磁图( 13 CNMR)
• MSDS 信息:4-Chloro-1-butanol(928-51-8).msds
• 毒性分级:中毒
• TCI Shanghai:4-氯-1-丁醇(含有数量不等的四氢呋喃) 4-Chloro-1-butanol (contains varying amounts of Tetrahydrofuran),>;85.0%(GC)(928-51-8)
• Acros Organics:4-氯-1-丁醇 4-Chloro-1-butanol, balance THF andHCl, 85%(928-51-8)
• 储运特性:库房低温通风干燥; 防明火, 防高温, 与氧化剂分开存放
• 类别:易燃液体
• 可燃性危险特性:遇热, 明火, 氧化剂燃烧; 热分解排出有毒氯化物烟雾
• MOL 文件:928-51-8.mol
• 用途二:用于有机合成。
• 用途一:用作有机合成中间体
• 海关编码:29055910
• 下游产品:1-(4-(吡咯烷-1-基)丁基)肼 --> 1-(4-吗啉基丁基)肼 --> 4-氨基-1-丁醇
• Hazard Note:Harmful
• 灭火剂:雾水,二氧化碳, 泡沫, 干粉