Iodomethane 碘甲烷

CAS 74-88-4 MFCD00001073

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产品品牌/编号/名称 纯度规格 包装 价格和现货
INFI H57220
Iodomethane 碘甲烷
99% 25g ¥ 52
库存 辽宁 保定市
中国国内现货 96-99 %
INFI H57220
Iodomethane 碘甲烷
99% 100g ¥ 136
库存 辽宁 保定市
中国国内现货 96-99 %
INFI H57220
Iodomethane 碘甲烷
99% 500g ¥ 440
库存 辽宁 保定市
中国国内现货 96-99 %
Innochem I00068
碘甲烷
100g ¥ 490
Purest P79337
碘甲烷
AR 100g ¥ 440
Innochem A04950
99% 25g ¥ 300
库存 北京
中国国内现货 96-99 %
Innochem A04950
99% 100g ¥ 490
96-99 %
Innochem A04950
99% 500g ¥ 1,350
96-99 %
Alfa 043681
Iodomethane
99+%, stab. with copper 50g ¥ 137
96-99 %
Alfa 043681
Iodomethane
99+%, stab. with copper 250g ¥ 1,438
96-99 %
Alfa 043681
Iodomethane
99+%, stab. with copper 1kg ¥ 4,600
96-99 %
Alfa H32660
Iodomethane
2M soln. in tert-butyl methyl ether 100mL ¥ 793
96-99 %
Alfa H32660
Iodomethane
2M soln. in tert-butyl methyl ether 500mL ¥ 2,236
96-99 %
Alfa 031876
Iodomethane
with copper 100g ¥ 357
99e1
Alfa 031876
Iodomethane
with copper 500g ¥ 1,176
99e1
Alfa A10559
Iodomethane
b. with copper or silver 50g ¥ 201
96-99 %
Alfa A10559
Iodomethane
b. with copper or silver 250g ¥ 667
96-99 %
Alfa A10559
Iodomethane
b. with copper or silver 1000g ¥ 2,125
96-99 %
Alfa 31876
Iodomethane
99.5%, stab. with copper 100g ¥ 360
99e1
Alfa 31876
Iodomethane
99.5%, stab. with copper 500g ¥ 1,186
99e1
Alfa 43681
Iodomethane
99+%, stab. with copper 50g ¥ 137
96-99 %
Alfa 43681
Iodomethane
99+%, stab. with copper 250g ¥ 510
96-99 %
Alfa 43681
Iodomethane
99+%, stab. with copper 1kg ¥ 1,935
96-99 %
TCI I0060
Iodomethane (stabilized with Copper chip) >
>99.5%(GC) 10mL ¥ 190
库存 上海市 北京 Tokyo, Japan
中国国内现货 96-99 %
TCI I0060
Iodomethane (stabilized with Copper chip) >
>99.5%(GC) 100mL ¥ 490
库存 上海市 北京 Tokyo, Japan
中国国内现货 96-99 %
TCI I0060
Iodomethane (stabilized with Copper chip) >
>99.5%(GC) 300mL ¥ 1,290
库存 上海市 北京 Tokyo, Japan
中国国内现货 96-99 %
J&K 395069
Iodomethane, 99%, stabilized with copper chip
99% 100g ¥ 395
库存 HB SH
中国国内现货 96-99 %
J&K 395069
Iodomethane, 99%, stabilized with copper chip
99% 500g ¥ 1,060
96-99 %
Supelco 506052
1item ¥ 348
库存 北京
中国国内现货
HY Y39137
Iodomethane 碘甲烷
99% 100g ¥ -
96-99 %
HY Y39137
Iodomethane 碘甲烷
99% 1kg ¥ -
96-99 %
TRC I708200
Iodomethane
5g ¥ 1,540
TRC I708200
Iodomethane
50g ¥ 2,100
Energy-chemical W610705
Iodomethane 碘甲烷
99.5% 25g ¥ 65
库存 上海市
中国国内现货 96-99 %
Energy-chemical W610705
Iodomethane 碘甲烷
99.5% 100g ¥ 180
库存 上海市
中国国内现货 96-99 %
Energy-chemical W610705
Iodomethane 碘甲烷
99.5% 500g ¥ 600
库存 上海市
中国国内现货 96-99 %
Energy-chemical W610705
Iodomethane 碘甲烷
99.5% 1kg ¥ 1,080
库存 上海市 北京市
中国国内现货 96-99 %
Energy-chemical W610750
Iodomethane 碘甲烷
99.5%,Energyseal 100g ¥ 200
库存 上海市 北京市
中国国内现货 96-99 %
Energy-chemical W610750
Iodomethane 碘甲烷
99.5%,Energyseal 500g ¥ 650
库存 上海市 北京市
中国国内现货 96-99 %
Aldrich 456756
100mL ¥ 1,199
3A A11097
Iodomethane 碘甲烷
99% 25g ¥ 80
96-99 %
3A A11097
Iodomethane 碘甲烷
99% 100g ¥ 210
96-99 %
3A A11097
Iodomethane 碘甲烷
99% 500g ¥ 750
库存 北京
中国国内现货 96-99 %
3A A11097
Iodomethane 碘甲烷
99% 1kg ¥ 1,390
96-99 %
Acros 122370025
99% 2.5kg ¥ 3,916
96-99 %
Acros 459010025
99% 2.5kg ¥ 5,479
96-99 %
Acros 378411000
2M solution in tert-Butyl methyl ether, AcroSeal? 100mL ¥ 747
2.0 M solution 甲基叔丁基醚
Acros 378418000
2M solution in tert-Butyl methyl ether, AcroSeal? 800mL ¥ 3,258
2.0 M solution 甲基叔丁基醚
Acros 122370050
99% 5g ¥ 264
96-99 %
Acros 122371000
99% 100g ¥ 390
96-99 %
Acros 459011000
99% 100g ¥ 486
96-99 %
Acros 122375000
99% 500g ¥ 1,047
96-99 %
Acros 459015000
99% 500g ¥ 1,770
96-99 %
Adamas 80880C
500g ¥ 565

分类

  • {SNA} Alkyl,
  • {SA} Alkyl, Analytical Standards, Analytical/Chromatography, Building Blocks, Chemical Synthesis, Chromatography, Environmental Standards, Halogenated Hydrocarbons, Nematicides,
  • {SNA} β-Glucuronidase Drug Analysis Bundle, Alkyl, Analytical and Industrial Enzymes, Building Blocks, Chemical Synthesis, Halogenated Hydrocarbons, IOD - Iodomethane, Organic Building Blocks, 生化试剂, 酶、抑制剂和底物
  • Alphabetic, Analytical Standards, Analytical/Chromatography, Chemical Class, Chromatography, Environmental Standards,

相关文献及参考

  • Merck 14 ,6087
  • Beil. 1 ,IV,87
  • Short: II/14a Title: Molecular Constants: Diamagnetic Molecules Author: Demaison, J.; Dubrulle, A.; Hüttner, W.; Tiemann, E. Editor: Hellwege, K.-H.; Hellwege, A.M. Source: Landolt-Börnstein, New Series Volume: II/14a Page: 1-788 Year: 1982 Keyword: organic compounds; molecular constants; spectroscopy; microwave spectroscopy ISBN: 3-540-11365-7 ISBN: 978-3-540-11365-2 Internet Resource: DOI:10.1007/b19966 RefComment: 196 figs., XI
  • Short: II/14b Title: Molecular Constants: Radicals, Diatomic Molecules and Substance Index Author: Brown, J.M.; Demaison, J.; Dubrulle, A.; Hüttner, W.; Tiemann, E. Editor: Hellwege, K.-H.; Hellwege, A.M. Source: Landolt-Börnstein, New Series Volume: II/14b Page: 1-373 Year: 1983 Keyword: organic compounds; molecular constants; spectroscopy; microwave spectroscopy; radicals ISBN: 3-540-11857-8 ISBN: 978-3-540-11857-2 Internet Resource: DOI:10.1007/b19967 RefComment: 196 figs., IX
  • Short: II/19a Title: Molecular Constants: Rotational, l-type, Centrifugal Distortion and Related Constants of Diamagnetic Diatomic, Linear, and Symmetric Top Molecules Author: Demaison, J.; Hüttner, W.; Tiemann, E.; Wlodarczak, G. Editor: Hüttner, W. Source: Landolt-Börnstein, New Series Volume: II/19a Year: 1992 Keyword: organic compounds; molecular constants; spectroscopy; microwave spectroscopy ISBN: 3-540-54409-7 ISBN: 978-3-540-54409-8 Internet Resource: DOI:10.1007/b42304 RefComment: XI, 143 pages. Abstract: Volume II/19 Molecular Constants mostly from Microwave, Molecular Beam and Sub-Doppler Laser Spectroscopy is a supplement to the earlier volumes II/4, II/6, and II/14. The slight change in the title reflects current trends in the applications of spectroscopic methods. Together, the four volumes collect all the critically evaluated data published up to 1989/90 on constants of free molecules obtained by classical and modern spectroscopy. Volume

安全信息

GHS Symbol
WGK Germany3
Hazard Codes
  • T
  • T,F,Xn
  • F;T
Hazard statements
  • H301 Toxic if swallowed 吞食有毒
  • H315 Causes skin irritation 会刺激皮肤
  • H331 Toxic if inhaled 吸入中毒
  • H312 Harmful in contact with skin 皮肤接触有害
  • H335 May cause respiratory irritation 可能导致呼吸道刺激
  • H351 Suspected of causing cancer 怀疑致癌
Personal Protective Equipment
  • Faceshields, full-face respirator (US), Gloves, Goggles, multi-purpose combination respirator cartridge (US)
Precautionary statements
  • P280 Wear protective gloves/protective clothing/eye protection/face protection. 戴防护手套/防护服/眼睛的保护物/面部保护物。
  • P271 Use only outdoors or in a well-ventilated area.? 只能在室外或通风良好的地方使用。
  • P264 Wash hands thoroughly after handling. 处理后要彻底洗净双手。
  • P301+310+330
  • P284 Wear respiratory protection.? 佩戴呼吸保护装置。
  • P201 Obtain special instructions before use. 使用前获取专门指示。
  • P501 Dispose of contents/container to..… 处理内容物/容器.....
  • P405 Store locked up. 上锁保管。
  • P308+311
  • P304+340+310
  • P270 Do not eat, drink or smoke when using this product. 使用本产品时不要吃东西,喝水或吸烟。
  • P260 Do not breathe dust/fume/gas/mist/vapours/spray. 不要吸入粉尘/烟/气体/烟雾/蒸汽/喷雾。
  • P202 Do not handle until all safety precautions have been read and understood. 已阅读并理解所有的安全预防措施之前,切勿操作。
  • P301+310 IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician. 如果食入:立即呼叫中毒控制中心或医生/医师。
  • P261 Avoid breathing dust/fume/gas/mist/vapours/spray. 避免吸入粉尘/烟/气体/烟雾/蒸汽/喷雾。
  • P311 Call a POISON CENTER or doctor/physician. 呼叫解毒中心或医生/医师。
  • P403+233 Store in a well-ventilated place. Keep container tightly closed. 存放在通风良好的地方。保持容器密闭。
Signal word
RTECSPA9450000
UN Number
  • UN2644
Risk Statements
Safety Statements
  • S45 In case of accident or if you feel unwell seek medical advice immediately (show the label where possible) 发生事故时或感觉不适时,立即求医(可能时出示标签);
  • S38 In case of insufficient ventilation wear suitable respiratory equipment 通风不良时,佩带适当的呼吸器;
  • S36/37 Wear suitable protective clothing and gloves 穿戴适当的防护服和手套;
  • S9 Keep container in a well-ventilated place 保持容器在通风良好的场所;
  • S16 Keep away from sources of ignition - No smoking 远离火源,禁止吸烟;
  • S24 Avoid contact with skin 避免皮肤接触;
Storage condition
  • Light Sensitive
  • Store at 0°C
Packing GroupI
Hazard Class6.1
Warnings
  • 危化品目录(2015)
TYPE OF TEST            : TDLo - Lowest published toxic dose
ROUTE OF EXPOSURE       : Subcutaneous
SPECIES OBSERVED        : Rodent - rat
DOSE/DURATION           : 50 mg/kg
TOXIC EFFECTS :
   Tumorigenic - equivocal tumorigenic agent by RTECS criteria
   Gastrointestinal - colon tumors
   Tumorigenic - tumors at site of application
REFERENCE :
   ZEKBAI Zeitschrift fuer Krebsforschung.  (Berlin, Fed. Rep. Ger.)  V.1-75,
   1903-71.  For publisher information, see JCROD7.  Volume(issue)/page/year:
   74,241,1970

TYPE OF TEST            : TDLo - Lowest published toxic dose
ROUTE OF EXPOSURE       : Intraperitoneal
SPECIES OBSERVED        : Rodent - mouse
DOSE/DURATION           : 44 mg/kg/8W-I
TOXIC EFFECTS :
   Tumorigenic - neoplastic by RTECS criteria
   Lungs, Thorax, or Respiration - tumors
REFERENCE :
   CNREA8 Cancer Research. (Public Ledger Building, Suit 816, 6th & Chestnut
   Sts., Philadelphia, PA 19106)  V.1-    1941-  Volume(issue)/page/year:
   35,1411,1975

TYPE OF TEST            : LC50 - Lethal concentration, 50 percent kill
ROUTE OF EXPOSURE       : Inhalation
SPECIES OBSERVED        : Rodent - mouse
DOSE/DURATION           : 5 gm/m3/57M-C
TOXIC EFFECTS :
   Details of toxic effects not reported other than lethal dose value
REFERENCE :
   BJIMAG British Journal of Industrial Medicine.  (British Medical Journal,
   Box 560B, Kennebunkport, ME 04046)  V.1-    1944-  Volume(issue)/page/year:
   7,122,1950

TYPE OF TEST            : LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE

TYPE OF TEST            : LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE       : Intraperitoneal
SPECIES OBSERVED        : Rodent - guinea pig
DOSE/DURATION           : 51 mg/kg
TOXIC EFFECTS :
   Details of toxic effects not reported other than lethal dose value
REFERENCE :
   85GMAT "Toxicometric Parameters of Industrial Toxic Chemicals Under Single
   Exposure," Izmerov, N.F., et al., Moscow, Centre of International Projects,
   GKNT, 1982  Volume(issue)/page/year: -,84,1982

TYPE OF TEST            : LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE       : Intraperitoneal
SPECIES OBSERVED        : Rodent - rat
DOSE/DURATION           : 101 mg/kg
TOXIC EFFECTS :
   Details of toxic effects not reported other than lethal dose value
REFERENCE :
   85GMAT "Toxicometric Parameters of Industrial Toxic Chemicals Under Single
   Exposure," Izmerov, N.F., et al., Moscow, Centre of International Projects,
   GKNT, 198

TYPE OF TEST            : LDLo - Lowest published lethal dose
ROUTE OF EXPOSURE       : Administration onto the skin
SPECIES OBSERVED        : Rodent - rabbit
DOSE/DURATION           : 794 mg/kg
TOXIC EFFECTS :
   Lungs, Thorax, or Respiration - other changes
   Gastrointestinal - other changes
   Blood - hemorrhage
REFERENCE :
   NTIS** National Technical Information Service.  (Springfield, VA 22161)
   Formerly U.

TYPE OF TEST            : Mutation in microorganisms
TEST SYSTEM             : Bacteria - Escherichia coli
DOSE/DURATION           : 20 umol/L
REFERENCE :
   ARTODN Archives of Toxicology.  (Springer-Verlag, Heidelberger Pl. 3, D-1000
   Berlin 33, Fed. Rep. Ger.)  V.32-    1974-  Volume(issue)/page/year:
   46,277,1980

TYPE OF TEST            : Mutation in mammalian somatic cells
TEST SYSTEM             : Rodent - hamster Ovary
DOSE/DURATION           : 2 mg/L
REFERENCE :
   MUREAV Mutation Research.  (Elsevier Science Pub. B.V., POB 211, 1000 AE
   Amsterdam, Netherlands) V.1-    1964-  Volume(issue)/page/year: 136,137,1984

TYPE OF TEST            : Mutation in microorganisms
TEST SYSTEM             : Rodent - mouse Lymphocyte
DOSE/DURATION           : 50 mg/L/4H
REFERENCE :
   MUREAV Mutation Research.  (Elsevier Science Pub. B.V., POB 211, 1000 AE
   Amsterdam, Netherlands) V.1-    1964-  Volume(issue)/page/year: 59,61,1979

TYPE OF

TYPE OF TEST            : DNA repair
TEST SYSTEM             : Bacteria - Escherichia coli
DOSE/DURATION           : 10 ug/disc
REFERENCE :
   JJIND8 JNCI, Journal of the National Cancer Institute.  (Washington, DC)
   V.61-79, 1978-87. For publisher information, see JNCIEQ.
   Volume(issue)/page/year: 62,873,1979

TYPE OF TEST            : Mutation in mammalian somatic cells
TEST SYSTEM             : Rodent - mouse Lymphocyte
DOSE/DURATION           : 3600 ug/L
REFERENCE :
   ENMUDM Environmental Mutagenesis.  (New York, NY)  V.1-9, 1979-87.  For
   publisher

TYPE OF TEST            : Gene conversion and mitotic recombination
TEST SYSTEM             : Yeast - Saccharomyces cerevisiae
DOSE/DURATION           : 1000 ppm
REFERENCE :
   JJIND8 JNCI, Journal of the National Cancer Institute.  (Washington, DC)
   V.61-79, 1978-87. For publisher information, see JNCIEQ.
   Volume(issue)/page/year: 62,901,1979

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其他信息

  • 实验室制备碘甲烷:在甲醇与红磷的混合物中加入碘时,会发生放热反应而生成碘甲烷:5 CH3OH + P + 2.5 I2 → 5 CH3I + H3PO4 + H2O 反应中生成了三碘化磷中间体,起到了与甲醇发生碘化反应的作用。 碘甲烷也可由硫酸二甲酯与碘化钾在碳酸钙存在下反应制得:(CH3O)2SO2 + KI → K2SO4 + 2 CH3I 先将反应产物蒸馏,然后用Na2S2O3、水和Na2CO3溶液洗涤,便可得到纯净的碘甲烷。
  • 外观性质:无色液体,有特臭。
  • MSDS 信息:碘甲烷(74-88-4).msds
  • {Chemicalbook
  • 用途二:用作分析试剂,也用于制药工业
  • 毒性分级:高毒
  • 下游产品:6-甲基-3-甲氧基-2-碘吡啶 --> 哌唑嗪 --> 4-甲基-2-甲硫基嘧啶 --> 2-甲基-5-甲氧基吡啶 --> 2,2-二甲基环戊酮 --> 克拉霉素 --> 2-甲硫基-4-氯-5-溴嘧啶 --> 2-甲基-2H-吲唑-3-甲酸 --> 2-甲硫基-4-苯甲氨基嘧啶 --> (S)-(-)-环氧丙基甲基醚 --> 2-甲硫基-4-氯嘧啶 --> 2-溴-3-甲氧基-6-甲基吡啶 --> 轻水泡沫灭火剂 FC-4 --> 4-氯-N-甲基嘧啶-2-胺 --> (1-甲基-1H-苯并眯唑-2-基)甲胺 --> 2,2-二甲基环己酮 --> 阿司咪唑 --> 3-甲基-4-硝基苯甲醚 --> (R)-(-)-环氧丙基甲基醚 --> 2-甲硫基-4,6-二甲基嘧啶 --> 7-甲氧基香豆素 --> 新戊基碘 --> 轻水泡沫灭火剂 FC-3 --> 1-(2-二甲基氨基乙基)-1H-5-巯基-四氮唑 --> 3Β,17Β-二羟基孕甾-5-烯-21-羧酸 --> 坎利酮 --> 2-苯基-2-丙醇 --> 3Β,17Β-二羟基孕甾-5-烯-21-羧酸-Γ-内酯 --> 美雄醇 --> 5-巯基-1,2,3,4-四氮唑-1-甲基磺酸 --> 2-乙酰基-3-甲基吡嗪 --> 3Β,17Β-二羟基雄甾-5-烯-17Α-丙炔酸 --> 碘化1,2-二甲基吡啶鎓 --> 雄甾-5-烯-3,17-二醇-17-丙炔酸钾盐 --> 苄基三甲基碘化铵
  • 图谱信息:碘甲烷(
  • Acros Organics:碘甲烷 Iodomethane,stabilized,99%(74-88-4)
  • F:8
  • 甲基化反应:碘甲烷与碳酸二甲酯、硫酸二甲酯、三氟甲磺酸甲酯是常见的甲基化试剂 根据软硬酸碱理论,碘是“软”的阴离子,因而碘甲烷所参与的甲基化反应也应在两位亲核试剂较“软”的一段发生。比如,在与硫氰酸根离子反应时,S更软,因而从S原子进攻的可能性较从N原子进攻的可能性大,产物主要是硫氰酸甲酯(CH3SCN)而非CH3NCS。而且,碘甲烷与1,3-二羰基化合物生成的烯醇盐之间发生的反应也可用以上理论来解释。相对于碳原子,氧原子较硬,碘甲烷参与的反应也几乎都生成C-甲基化的产物。 碘甲烷甲基化具有以下一些缺点: 它相对分子质量较大,一摩尔MeI的质量几乎等于三摩尔CH3Cl的质量; 碘化合物较氯化物和溴化物仍显得比较昂贵,因而在工业上更加便宜的硫酸二甲酯仍有不少应用,尽管它的毒性比碘甲烷要高出很多; 碘离子离去基团可能会造成副反应; 碘甲烷的毒性比相应的氯化合物和溴化合物要大,对生产工人很不利。 因此在选择甲基化试剂时,通常要均衡考虑价格、来源、毒性、化学选择性及反应容易程度等诸多因素。
  • 用途一:主要用作甲基化试剂,在医药工业中用于碘甲基蛋氨酸(维生素U)、镇痛药、解毒药磷酸系药物的生产
  • 概述:碘甲烷是一个卤代烃,分子式为CH3I、MeI,是甲烷的一碘取代物。沸点42.4℃,相对密度2.279(20/4℃),室温下为密度大的挥发性液体,偶极矩1.59D,折射率1.5304(20°C、D)、1.5293(21°C、D)。碘甲烷可与常见的有机溶剂混溶,微溶于水,溶于乙醇、乙醚,纯品无色,特臭,暴露于阳光下会分解出I2而带紫色,可通过加入金属铜
  • 急性毒性:吸入-大鼠LC50: 1300毫克/立方米/4小时; 腹腔-小鼠LD50:172 毫克/ 公斤
  • 用途三:医药工业用于碘甲基蛋氨酸(维生素U)、镇痛

化学结构图

CAS 74-88-4  MFCD00001073
SMILES: CI

化学属性

Mol. FormulaCH3I
Mol. Weight141.94
Density2.28
Refractive index1.5280 to 1.5330
Melting Point-64
TSCAYes
Boiling Point41-43
Vapor Density4.89 (vs air)
Vapor Pressure24.09 psi ( 55 °C)
Flash Point-28 ºC
Solubility14 G/L (20 ºC)

别名和识别编码

Chemical NameIodomethane
Synonym
  • Halon 10001
  • Joodmethaan
  • halon10001
  • Methane,iodo-
  • Iodometano
  • Metylu jodek
  • 碘甲烷
  • Methyliodide(CH3I)
  • ioduredemethyle(french)
  • Methyliodid
  • Methyl iodide
  • iodo-methan
  • 10domethane
  • Methane, iodo-
  • 碘化甲碘
  • Iodmethan
  • CH3I
  • METHYL IODIDE
  • 碘甲烷 IODOMETHANE
  • Monoioduro di metile
  • 碘甲烷 095-01 [6]
  • Methyliodide
  • 碘甲烷, 99%, 与铜或银稳定
  • 5-Iodoisatin
  • Iodomethane
  • ioduredemethyle
  • Monoiodomethane
  • RCRA waste number U138
    CAS Number74-88-4
    Beilstein Registry Number969135
    MDL NumberMFCD00001073
    EC Number200-819-5
    Merck Number6087
    PubChem Substance ID6328
    Chemical Name Translation碘甲烷
    Wiswesser Line NotationI1
    LabNetwork Molecule IDLN00196692
    Reaxys-RN969135
    InChIInChI=1S/CH3I/c1-2/h1H3

    系列性分类


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